4-nitrobenzoic acid tetramethylammonium salt

Base Information

• Chemical Name: 4-nitrobenzoic acid tetramethylammonium salt
• CAS No.: 53531-13-8
• Molecular Formula: C₄H₁₂N*C₇H₄NO₄
• Molecular Weight: 240.259
• Mol file: 53531-13-8.mol

Synonyms:4-nitrobenzoic acid tetramethylammonium salt

Chemical Property of 4-nitrobenzoic acid tetramethylammonium salt

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-nitrobenzoic acid tetramethylammonium salt

There total 2 articles about 4-nitrobenzoic acid tetramethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-dimethyl-formamide dimethyl acetal (4637-24-5) + 4-nitro-benzoic acid (62-23-7) → 4-nitrobenzoic acid methyl ester (619-50-1) + 4-nitrobenzoic acid tetramethylammonium salt (53531-13-8)

Guidance literature:

In 1,2-dichloro-ethane; at 24 ℃; for 69h;

DOI:10.1055/s-2008-1077882

Reference yield:

4-nitrobenzoic acid methyl ester (619-50-1) + trimethylamine (75-50-3) → 4-nitrobenzoic acid tetramethylammonium salt (53531-13-8)

Guidance literature:

In methanol; at 139.9 - 149.9 ℃; for 100h; Kinetics; Thermodynamic data; ΔH_excit., ΔS_excit.;

Reference yield:

4-nitrobenzoic acid tetramethylammonium salt (53531-13-8) + methyl iodide (74-88-4) → 4-nitrobenzoic acid methyl ester (619-50-1)

Guidance literature:

In acetonitrile; at 30 ℃; Kinetics; Thermodynamic data;

DOI:10.1039/b203032m

upstream raw materials:

4-nitrobenzoic acid methyl ester

trimethylamine

N,N-dimethyl-formamide dimethyl acetal

4-nitro-benzoic acid

Downstream raw materials:

ethyl 4-nitrobenzoate

4-nitrobenzoic acid methyl ester