2,2-dimethylcyclohexylcarboxaldehyde

Base Information

Chemical Name:2,2-dimethylcyclohexylcarboxaldehyde
CAS No.:13155-56-1
Molecular Formula:C₉H₁₆O
Molecular Weight:140.225
Hs Code.:

Synonyms:2,2-dimethylcyclohexylcarboxaldehyde

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Chemical Property of 2,2-dimethylcyclohexylcarboxaldehyde

Chemical Property:

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Technology Process of 2,2-dimethylcyclohexylcarboxaldehyde

There total 13 articles about 2,2-dimethylcyclohexylcarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2979-10-4
ethyl 2,2-dimethyl-6-oxocyclohexane-1-carboxylate

: 13155-56-1
2,2-dimethylcyclohexylcarboxaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / diethyl ether; mineral oil / 0.5 h / -20 °C

1.2: 1 h / -30 - 20 °C

2.1: triethylsilane / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 20 - 60 °C / Inert atmosphere

3.1: hydrogen / methanol / 20 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -30 °C / Inert atmosphere

4.2: 20 °C

5.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With triethylsilane; lithium aluminium tetrahydride; hydrogen; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 583-60-8
2-Methylcyclohexanone

: 13155-56-1
2,2-dimethylcyclohexylcarboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KH, triethylborane / 1.) THF, 12 h, 25 deg C; 2.) 10 h, THF

2: 1.) Me₃SiCH(Li)OMe / 1.) 25 deg C, overnight; 2.) 15 min; 2 h, reflux

With triethyl borane; lithium methoxy(trimethylsilyl)methylide; potassium hydride;
DOI:10.1021/ja00305a012

Reference yield:

: 1257045-68-3
ethyl {6,6-dimethyl-2-(trifluoromethanesulfonyloxy)cyclohexene-1-yl}carboxylate

: 13155-56-1
2,2-dimethylcyclohexylcarboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylsilane / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 2 h / 20 - 60 °C / Inert atmosphere

2.1: hydrogen / methanol / 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -30 °C / Inert atmosphere

3.2: 20 °C

4.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With triethylsilane; lithium aluminium tetrahydride; hydrogen; sodium hydrogencarbonate; Dess-Martin periodane; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;