[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

Base Information

Chemical Name:[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine
CAS No.:1005514-91-9
Molecular Formula:C₁₁H₁₅BrF₅NO₂S
Molecular Weight:400.208
Hs Code.:

Synonyms:[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

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Chemical Property of [3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

Chemical Property:

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Technology Process of [3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

There total 4 articles about [3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1005514-89-5
[3-(1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]dimethylamine

: 1005514-91-9
[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

: 1005514-90-8
[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]dimethylamine

Guidance literature:: With phenyltrimethyl tribromide; In tetrahydrofuran; methanol; at 60 ℃;

Reference yield:

: 1005514-86-2
3-dimethylamino-5-pentafluorosulfanylbenzoic acid

: 1005514-91-9
[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / dichloromethane / 5 h / 20 °C / Reflux; Inert atmosphere

1.2: 1 h / Inert atmosphere

2.1: diethyl ether; tetrahydrofuran / 0 - 25 °C / Inert atmosphere

2.2: Cooling; Inert atmosphere

3.1: camphor-10-sulfonic acid / methanol / Inert atmosphere

4.1: phenyltrimethylammonium tribromide / tetrahydrofuran; methanol / 60 °C / Inert atmosphere

With thionyl chloride; phenyltrimethylammonium tribromide; camphor-10-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;

Reference yield:

: 1005514-87-3
3-dimethylamino-N-methoxy-N-methyl-5-pentafluorosulfanylbenzamide

: 1005514-91-9
[3-(2-bromo-1,1-dimethoxyethyl)-5-pentafluorosulfanylphenyl]methylamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethyl ether; tetrahydrofuran / 0 - 25 °C / Inert atmosphere

1.2: Cooling; Inert atmosphere

2.1: camphor-10-sulfonic acid / methanol / Inert atmosphere

3.1: phenyltrimethylammonium tribromide / tetrahydrofuran; methanol / 60 °C / Inert atmosphere

With phenyltrimethylammonium tribromide; camphor-10-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether;