3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

Base Information

Chemical Name:3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one
CAS No.:40357-47-9
Molecular Formula:C17H15NO2
Molecular Weight:265.3065
Hs Code.:2933790090
Mol file:40357-47-9.mol

Synonyms:3-methoxy-1-methyl-4-phenyl-quinolin-2-one;3-methoxy-1-methyl-4-phenylquinolin-2(1h)-one;3-Methoxy-1-methyl-4-phenyl-1H-chinolin-2-on;3-Methoxy-1-methyl-4-phenylcarbostyril;3-methoxy-1-methyl-4-phenyl-1H-quinolin-2-one;N,3-O-Dimethylviridicatin;3-Methoxy-N-methyl-4-phenylcarbostyril;O,N-Dimethyl-viridicatin;

Suppliers and Price of 3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

Chemical Property:

Vapor Pressure:9.26E-07mmHg at 25°C
Boiling Point:404.7°C at 760 mmHg
Flash Point:198.6°C
PSA：31.23000
Density:1.22g/cm³
LogP:3.21410

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

There total 5 articles about 3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 129-24-8
4-phenyl-3-hydroxyquinolin-2(1H)-one

: 77-78-1
dimethyl sulfate

: 40357-47-9
3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1021/acs.orglett.8b01417

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 40357-47-9
3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid hydrazide; potassium carbonate / ethanol / 8 h / 80 °C

2: sodium hydroxide / tetrahydrofuran; water / 12 h / 20 °C

With potassium carbonate; toluene-4-sulfonic acid hydrazide; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/acs.orglett.8b01417

Reference yield:

: 100-52-7
benzaldehyde

: 40357-47-9
3-methoxy-1-methyl-4-phenylquinolin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid hydrazide; potassium carbonate / ethanol / 8 h / 80 °C

2: sodium hydroxide / tetrahydrofuran; water / 12 h / 20 °C

With potassium carbonate; toluene-4-sulfonic acid hydrazide; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/acs.orglett.8b01417