(10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide

Base Information

• Chemical Name: (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide
• CAS No.: 1429061-80-2
• Molecular Formula: Br*C₃₇H₃₈O₂PS₃
• Molecular Weight: 721.783
• Mol file: 1429061-80-2.mol

Synonyms:(10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide

Chemical Property of (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide

There total 3 articles about (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

desmethyl anethole trithione (18274-81-2) + 10-bromodecanoic acid (50530-12-6) + triphenylphosphine (603-35-0) → (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide (1429061-80-2)

Guidance literature:

10-bromodecanoic acid; triphenylphosphine; In acetonitrile; for 70h; Reflux;

desmethyl anethole trithione; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 22h;

Reference yield: 73.0%

(9-carboxynonyl)triphenylphosphonium bromide (93943-65-8) + 4-(4-hydroxyphenyl)-3H-1,2-dithiole-3-thione (28530-47-4) → (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide (1429061-80-2)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; for 22h;

Reference yield:

desmethyl anethole trithione (18274-81-2) + (9-carboxynonyl)triphenylphosphonium bromide (93943-65-8) → (10-oxo-10-(4-(3-thioxo-3H-1,2-dithiol-5-yl)phenoxy)decyl)triphenylphosphonium bromide (1429061-80-2)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 22h;

DOI:10.1039/c3md00323j

upstream raw materials:

(9-carboxynonyl)triphenylphosphonium bromide

4-(4-hydroxyphenyl)-3H-1,2-dithiole-3-thione

desmethyl anethole trithione

10-bromodecanoic acid