{[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

Base Information

Chemical Name:{[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)
CAS No.:1116460-24-2
Molecular Formula:C₂₀H₃₇BrO₃Si₂
Molecular Weight:461.587
Hs Code.:

Synonyms:{[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

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Chemical Property of {[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

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Technology Process of {[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

There total 4 articles about {[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1116460-22-0
{2,3-bis[(tert-butyldimethylsilyl)oxy]-4-methoxyphenyl}methanol

: 1116460-24-2
{[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 ℃; for 15h; Inert atmosphere;
DOI:10.1016/j.tet.2020.131619

Reference yield:

: 4055-69-0
2,3-dihydroxy-4-methoxybenzaldehyde

: 1116460-24-2
{[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 0 °C / Inert atmosphere

2: sodium tetrahydroborate; ethanol / 0.5 h / 0 - 20 °C

3: phosphorus tribromide / dichloromethane / 15 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; ethanol; phosphorus tribromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2020.131619

Reference yield:

: 109971-66-6
2,3-bis<(tert-butyldimethylsilyl)oxy>-4-methoxybenzaldehyde

: 1116460-24-2
{[3-(bromomethyl)-6-methoxy-1,2-phenylene] bis(oxy)}bis(tert-butyldimethylsilane)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; ethanol / 0.5 h / 0 - 20 °C

2: phosphorus tribromide / dichloromethane / 15 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; ethanol; phosphorus tribromide; In dichloromethane;
DOI:10.1016/j.tet.2020.131619