Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

Base Information

Chemical Name:Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester
CAS No.:100548-98-9
Molecular Formula:C₁₇H₂₅NO₅S
Molecular Weight:355.455
Hs Code.:

Synonyms:Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

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Chemical Property of Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

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Technology Process of Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

There total 5 articles about Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.4%

: 75-36-5
acetyl chloride

: 160114-16-9,160114-21-6,94057-02-0
2-{4-(3-ethoxy-2-hydroxypropoxy)phenylcarbamoyl}ethyl methyl sulfide

: 100548-98-9
Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

Guidance literature:: With pyridine; In benzene; for 3h; Ambient temperature;
DOI:10.1021/jm970285z

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 100548-98-9
Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) pyridine, 2.) aq. KOH / 1.) 90 deg C, 6 h, 2.) acetone, RT, 2 h

2: H₂SO₄ / 6 h / 80 °C

3: H₂ / 10percent Pd/C / ethanol / 8 h / Ambient temperature

4: Et₃N / CH₂Cl₂ / 3 h / 10 °C

5: 76.4 percent / pyridine / benzene / 3 h / Ambient temperature

With pyridine; potassium hydroxide; sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; benzene;
DOI:10.1021/jm970285z

Reference yield:

: 125228-75-3
4-nitrophenyl 2-oxiranylmethyl ether

: 100548-98-9
Acetic acid 1-ethoxymethyl-2-[4-(3-methylsulfanyl-propionylamino)-phenoxy]-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄ / 6 h / 80 °C

2: H₂ / 10percent Pd/C / ethanol / 8 h / Ambient temperature

3: Et₃N / CH₂Cl₂ / 3 h / 10 °C

4: 76.4 percent / pyridine / benzene / 3 h / Ambient temperature

With pyridine; sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; benzene;
DOI:10.1021/jm970285z