C₅₄H₈₈N₂O₉Si₃

Base Information

Chemical Name:C₅₄H₈₈N₂O₉Si₃
CAS No.:1308253-77-1
Molecular Formula:C₅₄H₈₈N₂O₉Si₃
Molecular Weight:993.557
Hs Code.:

C<sub>54</sub>H<sub>88</sub>N<sub>2</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₅₄H₈₈N₂O₉Si₃

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Chemical Property of C₅₄H₈₈N₂O₉Si₃

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Technology Process of C₅₄H₈₈N₂O₉Si₃

There total 11 articles about C₅₄H₈₈N₂O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1308253-70-4
C₃₆H₄₆N₂O₉

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1308253-77-1
C₅₄H₈₈N₂O₉Si₃

Guidance literature:: With triethylamine; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1002/jhet.609

Reference yield:

: 1177255-28-5
(S)-methyl-2-acetamido-3-(3-hydroxy-4-methoxy-5-methylphenyl)propanoate

: 1308253-77-1
C₅₄H₈₈N₂O₉Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: lithium borohydride / tetrahydrofuran / 24 h

2: hydrogenchloride / methanol; water / 6 h / Reflux

3: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 9 h / -10 °C / Molecular sieve

4: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 - 20 °C

5: triethylamine; trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With hydrogenchloride; lithium borohydride; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1002/jhet.609

Reference yield:

: C₁₅H₁₉NO₆

: 1308253-77-1
C₅₄H₈₈N₂O₉Si₃

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; water / methanol / 10 h

2: lithium borohydride / tetrahydrofuran / 24 h

3: hydrogenchloride / methanol; water / 6 h / Reflux

4: acetic acid / dichloromethane; 2,2,2-trifluoroethanol / 9 h / -10 °C / Molecular sieve

5: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine / dichloromethane / 0 - 20 °C

6: triethylamine; trifluoroacetic acid / dichloromethane / 24 h / 20 °C

With hydrogenchloride; lithium borohydride; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol; water;
DOI:10.1002/jhet.609