3-Triisopropylsilyl-2-propyn-1-OL

Base Information

• Chemical Name: 3-Triisopropylsilyl-2-propyn-1-OL
• CAS No.: 104493-07-4
• Molecular Formula: C₁₂H₂₄OSi
• Molecular Weight: 212.407
• DSSTox Substance ID: DTXSID101267086

Synonyms:104493-07-4;3-tri(propan-2-yl)silylprop-2-yn-1-ol;3-TRIISOPROPYLSILYL-2-PROPYN-1-OL;3-(Triisopropylsilyl)propargyl alcohol;SCHEMBL4447362;DTXSID101267086;3-(triisopropylsilyl)prop-2-yn-1-ol;AKOS037652998;FS-6338;3-[Tris(1-methylethyl)silyl]-2-propyn-1-ol

Chemical Property of 3-Triisopropylsilyl-2-propyn-1-OL

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 212.159641919
• Heavy Atom Count: 14
• Complexity: 207

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)[Si](C#CCO)(C(C)C)C(C)C

Technology Process of 3-Triisopropylsilyl-2-propyn-1-OL

There total 1 articles about 3-Triisopropylsilyl-2-propyn-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triiso-propyl(3-(4-methoxybenzyloxy)prop-1-ynyl)silane → 3-(triisopropylsilyl)propargyl alcohol (104493-07-4) + 4-methoxy-benzaldehyde (123-11-5)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 0 - 20 ℃; for 3.25h; Inert atmosphere;

DOI:10.1002/chem.201001539

Reference yield: 95.0%

3-(triisopropylsilyl)propargyl alcohol (104493-07-4) + 4-Nitrophenyl chloroformate (7693-46-1) → C19H27NO5Si

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 16h; Cooling with ice;

Reference yield: 92.0%

N-[(4,5-dimethylcyclohexa-1,4-dienyl)methyl]-4-methylbenzenesulfonamide (873424-55-6) + 3-(triisopropylsilyl)propargyl alcohol (104493-07-4) → N-((4,5-dimethylcyclohexa-1,4-dienyl)methyl)-4-methyl-N-(3-(triisopropylsilyl)-prop-2-ynyl)benzenesulfonamide

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran;

DOI:10.1021/ol061801v

Downstream raw materials:

3-triisopropylsilyl-2-propynal

1-nitro-2-(prop-2-yn-1-yloxy)benzene

1-(triisopropylsilyl)-5-(trimethylsilyl)penta-1,4-diyn-3-ol

3-[(tert-butylcyclohex-1-enyl)ethynyl]-1-(triisopropylsilyl)-5-(trimethylsilyl)penta-1,4-diyn-3-ol

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