phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester

Base Information

• Chemical Name: phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester
• CAS No.: 170502-11-1
• Molecular Formula: C₁₈H₂₆O₂S
• Molecular Weight: 306.469
• Mol file: 170502-11-1.mol

Synonyms:phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester

Chemical Property of phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester

There total 3 articles about phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(phenylthio)acetic acid chloride (7031-27-8) + (-)-menthol (2216-51-5) → phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester (170502-11-1)

Guidance literature:

With pyridine; Ambient temperature;

DOI:10.1016/0022-1139(94)03207-G

Reference yield: 59.0%

(-)-menthol (2216-51-5) + (phenylthio)acetic acid (103-04-8) → phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester (170502-11-1)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.166667h;

DOI:10.1080/00397911.2018.1554145

Reference yield: 52.0%

benzenesulfinyl-acetic acid 2'-isopropyl-5'-methylcyclohexyl ester + allyl-trimethyl-silane (762-72-1) → phenylsulfanyl-acetic acid 2'-isopropyl-5'-methyl-cyclohexyl ester (170502-11-1) + 2-Phenylsulfanyl-pent-4-enoic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

Guidance literature:

With trifluoroacetic anhydride; In dichloromethane; at -78 ℃; for 2h;

DOI:10.1016/S0040-4039(00)00681-X

upstream raw materials:

(phenylthio)acetic acid chloride

(-)-menthol

allyl-trimethyl-silane

(phenylthio)acetic acid

Downstream raw materials:

(-)-menthyloxycarbonyl-α-(phenylthio)methyl chloride