4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Base Information

Chemical Name:4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester
CAS No.:256530-69-5
Molecular Formula:C₂₂H₂₂N₄O₆
Molecular Weight:438.44
Hs Code.:

Synonyms:4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

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Chemical Property of 4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

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Technology Process of 4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

There total 5 articles about 4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 256530-63-9
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

: 256530-69-5
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: With cerium(IV) ammonium nitrate; In acetone; at 20 ℃; for 0.333333h;

Reference yield:

: 21731-17-9
methyl 3-aminocrotonate

: 256530-69-5
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / acetic acid / 22 h / 20 - 60 °C

2: 90 percent / aq. [(NH₄)2Ce](NO₃)6 / acetone / 0.33 h / 20 °C

With cerium(IV) ammonium nitrate; In acetic acid; acetone; 1: cyclocondensation; Hantzsch synthesis / 2: Dehydrogenation;

Reference yield:

: 13230-06-3
2-Methyl-4-nitro-1-(phenylmethyl)-1H-imidazole

: 256530-69-5
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / KOtBu / tetrahydrofuran; dimethylformamide / 0.17 h / -70 °C

2: 60 percent / AgNO₃; H₂O / toluene / 2.5 h / Heating

3: 65 percent / acetic acid / 22 h / 20 - 60 °C

4: 90 percent / aq. [(NH₄)2Ce](NO₃)6 / acetone / 0.33 h / 20 °C

With cerium(IV) ammonium nitrate; potassium tert-butylate; water; silver nitrate; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; acetone; toluene; 1: Substitution / 2: Hydrolysis / 3: cyclocondensation; Hantzsch synthesis / 4: Dehydrogenation;