4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Base Information

Chemical Name:4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester
CAS No.:256530-63-9
Molecular Formula:C₂₂H₂₄N₄O₆
Molecular Weight:440.456
Hs Code.:

Synonyms:4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

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Chemical Property of 4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

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Technology Process of 4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

There total 3 articles about 4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 21731-17-9
methyl 3-aminocrotonate

: 256530-60-6
1-Benzyl-2-methyl-4-nitroimidazol-5-carbaldehyd

: 256530-63-9
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: In acetic acid; at 20 - 60 ℃; for 22h;

Reference yield:

: 13230-06-3
2-Methyl-4-nitro-1-(phenylmethyl)-1H-imidazole

: 256530-63-9
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / KOtBu / tetrahydrofuran; dimethylformamide / 0.17 h / -70 °C

2: 60 percent / AgNO₃; H₂O / toluene / 2.5 h / Heating

3: 65 percent / acetic acid / 22 h / 20 - 60 °C

With potassium tert-butylate; water; silver nitrate; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; toluene; 1: Substitution / 2: Hydrolysis / 3: cyclocondensation; Hantzsch synthesis;

Reference yield:

: 256530-58-2
1-Benzyl-5-dichlormethyl-2-methyl-4-nitroimidazol

: 256530-63-9
4-(1-Benzyl-2-methyl-4-nitro-imidazol-5-yl)-1,4-dihydro-2,6-dimethyl-pyridin-3,5-dicarbonsaeuredimethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / AgNO₃; H₂O / toluene / 2.5 h / Heating

2: 65 percent / acetic acid / 22 h / 20 - 60 °C

With water; silver nitrate; In acetic acid; toluene; 1: Hydrolysis / 2: cyclocondensation; Hantzsch synthesis;