Iodomethyl-1-cyclohexane carboxylate

Base Information

Chemical Name:Iodomethyl-1-cyclohexane carboxylate
CAS No.:84089-33-8
Molecular Formula:C₈H₁₃IO₂
Molecular Weight:268.095
Hs Code.:

Synonyms:Iodomethyl-1-cyclohexane carboxylate

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Chemical Property of Iodomethyl-1-cyclohexane carboxylate

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Technology Process of Iodomethyl-1-cyclohexane carboxylate

There total 3 articles about Iodomethyl-1-cyclohexane carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29916-48-1
chloromethyl cyclohexanoic acid ester

: 84089-33-8
Iodomethyl-1-cyclohexane carboxylate

Guidance literature:: With 18-crown-6 ether; sodium iodide; In benzene; Heating;
DOI:10.1016/S0960-894X(99)00316-9

Reference yield:

: 2719-27-9
cyclohexanylcarbonyl chloride

: 84089-33-8
Iodomethyl-1-cyclohexane carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: ZnCl₂

2: NaI, 18-crown-6 / benzene / Heating

With 18-crown-6 ether; sodium iodide; zinc(II) chloride; In benzene;
DOI:10.1016/S0960-894X(99)00316-9

Reference yield:

: 98-89-5
Cyclohexanecarboxylic acid

: 84089-33-8
Iodomethyl-1-cyclohexane carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / water; dichloromethane / 4 h / 20 °C / Inert atmosphere

2: sodium iodide / acetone / 24 h / 20 °C

With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; sodium iodide; In dichloromethane; water; acetone;
DOI:10.1002/cbic.201300085