phenylthiomethyl cyclohexanecarboxylate

Base Information

Chemical Name:phenylthiomethyl cyclohexanecarboxylate
CAS No.:134281-47-3
Molecular Formula:C₁₄H₁₈O₂S
Molecular Weight:250.362
Hs Code.:

Synonyms:phenylthiomethyl cyclohexanecarboxylate

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Chemical Property of phenylthiomethyl cyclohexanecarboxylate

Chemical Property:

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Technology Process of phenylthiomethyl cyclohexanecarboxylate

There total 2 articles about phenylthiomethyl cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 882-33-7
diphenyldisulfane

: 84089-33-8
Iodomethyl-1-cyclohexane carboxylate

: 134281-47-3
phenylthiomethyl cyclohexanecarboxylate

Guidance literature:: Iodomethyl-1-cyclohexane carboxylate; With isopropylmagnesium chloride; In tetrahydrofuran; at -78 ℃; for 0.25h;

diphenyldisulfane; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1055/s-1999-2935

Reference yield:

: 7205-91-6
phenylthiomethyl chloride

: 98-89-5
Cyclohexanecarboxylic acid

: 134281-47-3
phenylthiomethyl cyclohexanecarboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene;
DOI:10.1016/S0040-4020(01)87075-7

Reference yield:

: 134281-47-3
phenylthiomethyl cyclohexanecarboxylate

: 98-89-5
Cyclohexanecarboxylic acid

Guidance literature:: With Bu₄NB₄; In water; acetonitrile; Yield given; Ambient temperature; electrolysis (electrodes of platinum sheet, 0.1 A constant current);
DOI:10.1016/S0040-4020(01)87075-7