chloromethyl cyclohexanoic acid ester

Base Information

• Chemical Name: chloromethyl cyclohexanoic acid ester
• CAS No.: 29916-48-1
• Molecular Formula: C₈H₁₃ClO₂
• Molecular Weight: 176.643
• Mol file: 29916-48-1.mol

Synonyms:chloromethyl cyclohexanoic acid ester

Chemical Property of chloromethyl cyclohexanoic acid ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chloromethyl cyclohexanoic acid ester

There total 3 articles about chloromethyl cyclohexanoic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

chlorosulfuric acid chloromethyl ester (49715-04-0) + Cyclohexanecarboxylic acid (98-89-5) → chloromethyl cyclohexanoic acid ester (29916-48-1)

Guidance literature:

With tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In dichloromethane; water; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1002/cbic.201300085

Reference yield: 36.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + cyclohexanylcarbonyl chloride (2719-27-9) → chloromethyl cyclohexanoic acid ester (29916-48-1)

Guidance literature:

With zinc(II) chloride; at 0 - 55 ℃;

DOI:10.1021/jm8011799

Reference yield:

→ chloromethyl cyclohexanoic acid ester (29916-48-1)

Guidance literature:

Cyclohexancarbonylchlorid;

DOI:10.1021/ja00723a018

upstream raw materials:

formaldehyd

cyclohexanylcarbonyl chloride

chlorosulfuric acid chloromethyl ester

Cyclohexanecarboxylic acid