4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide
CAS No.:1360897-76-2
Molecular Formula:C₂₃H₃₄N₂O₃S
Molecular Weight:418.601
Hs Code.:

Synonyms:4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

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Chemical Property of 4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

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Technology Process of 4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

There total 4 articles about 4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.9%

: 1360897-57-9
2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethyl 4-methylbenzenesulfonate

: 174291-96-4,58825-94-8
(1R,2R)-(-)-N-p-tosyl-1,2-cyclohexanediamine

: 1360897-76-2
4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; potassium iodide; In toluene; at 135 ℃; for 20h;

Reference yield:

: 3973-18-0
2-(prop-2-ynyloxy)ethanol

: 98-59-9
p-toluenesulfonyl chloride

: 174291-96-4,58825-94-8
(1R,2R)-(-)-N-p-tosyl-1,2-cyclohexanediamine

: 78-79-5,9003-31-0
isoprene

: 1360897-76-2
4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

Guidance literature:: 2-(prop-2-ynyloxy)ethanol; isoprene; With 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc; In tetrahydrofuran; at 35 ℃; for 1h;

p-toluenesulfonyl chloride; With 1-methyl-1H-imidazole; triethylamine; In toluene; at 20 ℃; for 1h;

(1R,2R)-(-)-N-p-tosyl-1,2-cyclohexanediamine; With N-ethyl-N,N-diisopropylamine; potassium iodide; In toluene; at 135 ℃; for 20h;

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 1360897-76-2
4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc(II) iodide; zinc / 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide / tetrahydrofuran / 1 h / 35 °C / Inert atmosphere

1.2: 1 h / 20 °C / Cooling with ice

2.1: potassium iodide; N-ethyl-N,N-diisopropylamine / toluene / 20 h / 135 °C

With N-ethyl-N,N-diisopropylamine; potassium iodide; zinc(II) iodide; zinc; 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; In tetrahydrofuran; toluene;