4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride

Base Information

Chemical Name:4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride
CAS No.:1360897-77-3
Molecular Formula:C₂₃H₃₄N₂O₃S*ClH
Molecular Weight:455.061
Hs Code.:

Synonyms:4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride

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Chemical Property of 4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride

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Technology Process of 4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride

There total 2 articles about 4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

: 1360897-76-2
4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide

: 1360897-77-3
4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; for 0.5h;

Reference yield:

: 3973-18-0
2-(prop-2-ynyloxy)ethanol

: 174291-96-4,58825-94-8
(1R,2R)-(-)-N-p-tosyl-1,2-cyclohexanediamine

: 78-79-5,9003-31-0
isoprene

: 1360897-77-3
4-methyl-N-((1R,2R)-2-(2-((4-methyl cyclohexa-1,4-dienyl)methoxy)ethylamino)cyclohexyl)benzenesulfonamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc / tetrahydrofuran / 1 h / 35 °C

1.2: 1 h / 20 °C

1.3: 20 h / 135 °C

2.1: hydrogenchloride / dichloromethane; methanol / 0.5 h

With hydrogenchloride; 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc; In tetrahydrofuran; methanol; dichloromethane;