4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

Base Information

Chemical Name:4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside
CAS No.:406225-39-6
Molecular Formula:C₂₁H₃₀O₈
Molecular Weight:410.464
Hs Code.:

Synonyms:4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

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Chemical Property of 4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

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Technology Process of 4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

There total 3 articles about 4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 406225-38-5
4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

: 406225-39-6
4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

Guidance literature:: 4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 0.75h;

With sodium hydroxide; dihydrogen peroxide; for 30h; Further stages.;

Reference yield:

: 333717-27-4
4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

: 406225-39-6
4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine

2.1: 9-BBN / tetrahydrofuran / 0.75 h / 20 °C

2.2: 90 percent / aq. H₂O₂; aq. NaOH / 30 h

With pyridine; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran;

Reference yield:

: 406225-37-4
5,6-anhydro-2,3-O-isopropylidene-1-O-(4-methoxybenzyl)-L-gulose

: 406225-39-6
4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 95 percent / CuI / tetrahydrofuran / 2 h / -30 - -10 °C

2.1: pyridine

3.1: 9-BBN / tetrahydrofuran / 0.75 h / 20 °C

3.2: 90 percent / aq. H₂O₂; aq. NaOH / 30 h

With pyridine; copper(l) iodide; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran;