4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Base Information

Chemical Name:4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside
CAS No.:333717-27-4
Molecular Formula:C₁₉H₂₆O₆
Molecular Weight:350.412
Hs Code.:

Synonyms:4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

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Chemical Property of 4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

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Technology Process of 4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

There total 3 articles about 4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 3536-96-7
vinylmagnesium chloride

: 406225-37-4
5,6-anhydro-2,3-O-isopropylidene-1-O-(4-methoxybenzyl)-L-gulose

: 333717-27-4
4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; at -30 - -10 ℃; for 2h;

Reference yield: 77.0%

: 333717-22-9
4-methoxybenzyl 2,3-O-isopropylidene-α-D-lyxo-pentodialdo-1,4-furanoside

: 762-72-1
allyl-trimethyl-silane

: 333717-23-0
(R)-1-[(3aS,4R,6S,6aS)-6-(4-Methoxy-benzyloxy)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl]-but-3-en-1-ol

: 333717-27-4
4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 2h;
DOI:10.1021/jo001447t

Reference yield: 70.0%

: 1826-67-1
vinyl magnesium bromide

: 406225-37-4
5,6-anhydro-2,3-O-isopropylidene-1-O-(4-methoxybenzyl)-L-gulose

: 333717-27-4
4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Guidance literature:: vinyl magnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -25 ℃; for 0.25h; Inert atmosphere;

5,6-anhydro-2,3-O-isopropylidene-1-O-(4-methoxybenzyl)-L-gulose; In tetrahydrofuran; at -25 - 20 ℃;
DOI:10.1002/ejoc.200801000