4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Base Information

Chemical Name:4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside
CAS No.:406225-38-5
Molecular Formula:C₂₁H₂₈O₇
Molecular Weight:392.449
Hs Code.:

Synonyms:4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

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Chemical Property of 4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

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Technology Process of 4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

There total 2 articles about 4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 406225-37-4
5,6-anhydro-2,3-O-isopropylidene-1-O-(4-methoxybenzyl)-L-gulose

: 406225-38-5
4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CuI / tetrahydrofuran / 2 h / -30 - -10 °C

2: pyridine

With pyridine; copper(l) iodide; In tetrahydrofuran;

Reference yield:

: 108-24-7
acetic anhydride

: 333717-27-4
4-methoxybenzyl 6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

: 406225-38-5
4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

Guidance literature:: With pyridine;

Reference yield: 90.0%

: 406225-38-5
4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside

: 406225-39-6
4-methoxybenzyl 5-O-acetyl-6,7-dideoxy-2,3-O-(1-methylethylidene)-α-D-manno-octofuraniside

Guidance literature:: 4-methoxybenzyl 5-O-acetyl-6,7,8,-trideoxy-2,3-O-(1-methylethylidene)-α-D-manno-oct-7-enofuraniside; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 0.75h;

With sodium hydroxide; dihydrogen peroxide; for 30h; Further stages.;