N'-phenylhydrazinecarbodithioic acid phenylethyl ester

Base Information

• Chemical Name: N'-phenylhydrazinecarbodithioic acid phenylethyl ester
• CAS No.: 1138320-45-2
• Molecular Formula: C₁₅H₁₆N₂S₂
• Molecular Weight: 288.437
• Mol file: 1138320-45-2.mol

Synonyms:N'-phenylhydrazinecarbodithioic acid phenylethyl ester

Chemical Property of N'-phenylhydrazinecarbodithioic acid phenylethyl ester

Chemical Property:

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Technology Process of N'-phenylhydrazinecarbodithioic acid phenylethyl ester

There total 3 articles about N'-phenylhydrazinecarbodithioic acid phenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

carbon disulfide (75-15-0,12122-00-8) + 2-phenylethyl tosylate (4455-09-8) + phenylhydrazine (100-63-0) → N'-phenylhydrazinecarbodithioic acid phenylethyl ester (1138320-45-2)

Guidance literature:

carbon disulfide; phenylhydrazine; With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

2-phenylethyl tosylate; In dimethyl sulfoxide; for 2.58333h;

DOI:10.1080/00397910802519141

Reference yield: 87.0%

carbon disulfide (75-15-0,12122-00-8) + 2-phenylethanol (60-12-8) + phenylhydrazine (100-63-0) → N'-phenylhydrazinecarbodithioic acid phenylethyl ester (1138320-45-2)

Guidance literature:

carbon disulfide; phenylhydrazine; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

2-phenylethanol; With triphenylphosphine; diethylazodicarboxylate; In dimethyl sulfoxide; at 20 ℃; for 2h; chemoselective reaction; Inert atmosphere;

DOI:10.1007/BF03249073

Reference yield: 86.0%

carbon disulfide (75-15-0,12122-00-8) + 2-phenylethyl chloride (622-24-2) + phenylhydrazine (100-63-0) → N'-phenylhydrazinecarbodithioic acid phenylethyl ester (1138320-45-2)

Guidance literature:

carbon disulfide; phenylhydrazine; With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 20 ℃; Inert atmosphere;

2-phenylethyl chloride; In dimethyl sulfoxide; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1007/s00706-008-0873-9

upstream raw materials:

carbon disulfide

2-phenylethyl tosylate

phenylhydrazine

2-phenylethyl chloride