2-methylallyl N-benzoyloxybenzimidothioate

Base Information

Chemical Name:2-methylallyl N-benzoyloxybenzimidothioate
CAS No.:1568950-81-1
Molecular Formula:C₁₈H₁₇NO₂S
Molecular Weight:311.404
Hs Code.:

Synonyms:2-methylallyl N-benzoyloxybenzimidothioate

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Chemical Property of 2-methylallyl N-benzoyloxybenzimidothioate

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Technology Process of 2-methylallyl N-benzoyloxybenzimidothioate

There total 4 articles about 2-methylallyl N-benzoyloxybenzimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 15177-34-1
thiobenzhydroxamic acid

: 98-88-4
benzoyl chloride

: 563-47-3
3-Chloro-2-methylpropene

: 1568950-81-1
2-methylallyl N-benzoyloxybenzimidothioate

Guidance literature:: thiobenzhydroxamic acid; 3-Chloro-2-methylpropene; With tetra-(n-butyl)ammonium iodide; triethylamine; In tetrahydrofuran; at 60 ℃;

benzoyl chloride; With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1021/jo500080x

Reference yield:

: 100-52-7
benzaldehyde

: 1568950-81-1
2-methylallyl N-benzoyloxybenzimidothioate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; sodium hydroxide / N,N-dimethyl-formamide; water / 1 h / 30 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.1: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

4.1: triethylamine; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 60 °C

4.2: 0.5 h / 20 °C

With sodium sulfide; N-chloro-succinimide; hydroxylamine hydrochloride; tetra-(n-butyl)ammonium iodide; triethylamine; sodium hydroxide; In tetrahydrofuran; diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jo500080x

Reference yield:

: 698-16-8
benzohydroximoyl chloride

: 1568950-81-1
2-methylallyl N-benzoyloxybenzimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium sulfide; triethylamine / diethyl ether; water / 1 h / 20 °C

2.1: triethylamine; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 60 °C

2.2: 0.5 h / 20 °C

With sodium sulfide; tetra-(n-butyl)ammonium iodide; triethylamine; In tetrahydrofuran; diethyl ether; water;
DOI:10.1021/jo500080x