2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one

Base Information

• Chemical Name: 2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one
• CAS No.: 200804-80-4
• Molecular Formula: C₁₅H₁₁N₃OS
• Molecular Weight: 281.338
• Mol file: 200804-80-4.mol

Synonyms:2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one

Chemical Property of 2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

(5E)-2-Mercapto-3-phenyl-5-(pyridin-2-ylmethylene)-3,5-dihydro-4H-imidazol-4-one ^*data from reagent suppliers

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Technology Process of 2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one

There total 1 articles about 2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

pyridine-2-carbaldehyde (1121-60-4) + 3-phenyl-2-thioxoimidazolidin-4-one (2010-15-3) → 2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one (200804-80-4)

Guidance literature:

With sodium acetate; acetic acid; for 2h; Heating;

DOI:10.1080/10426509708043491

Reference yield: 93.0%

ethyl bromoacetate (105-36-2) + 2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one (200804-80-4) → (5Z)-5-(pyridin-2-ylmethylidene)-3-phenyl-2-(carbethoxymethylthio)-4,5-dihydro-4H-imidazol-4-one (1224692-33-4)

Guidance literature:

2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one; With potassium hydroxide; In ethanol; water;

ethyl bromoacetate; In ethanol; water; for 3h;

DOI:10.1134/S1070363209070172

Reference yield: 86.0%

2-thioxo-3-phenyl-5-(pyridine-2-ylmethylene)-3,5-dihydro-4H-imidazole-4-one (200804-80-4) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-{5-oxo-1-phenyl-4-[1-pyridin-2-yl-meth-(Z)-ylidene]-4,5-dihydro-1H-imidazol-2-ylsulfanyl}-tetrahydro-pyran-3-yl ester

Guidance literature:

With potassium hydroxide; In acetone; for 6h; Ambient temperature;

DOI:10.1080/10426509708043491

upstream raw materials:

pyridine-2-carbaldehyde

3-phenyl-2-thioxoimidazolidin-4-one

Downstream raw materials:

(5Z)-5-(pyridin-2-ylmethylidene)-3-phenyl-2-(carbethoxymethylthio)-4,5-dihydro-4H-imidazol-4-one

2-methylthio-5-(2-pyridyl)methylene-3-phenyl-3,5-dihydro-4H-imidazol-4-one

Cu((5Z)-2-methylthio-3-phenyl-5-(α-pyridylmethylidene)-3,5-dihydro-4H-imidazol-4-one)Cl2

methyl 2-[[(4Z)-5-oxo-1-phenyl-4-(2-pyridylmethylene)-4,5-dihydro-1H-imidazol-2-yl]thio]-propionate

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