4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

Base Information

Chemical Name:4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid
CAS No.:1204336-23-1
Molecular Formula:C₂₀H₂₄ClN₃O₃
Molecular Weight:389.882
Hs Code.:

Synonyms:4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

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Chemical Property of 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

Chemical Property:

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Technology Process of 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

There total 1 articles about 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1204316-03-9
4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid methyl ester

: 1204336-23-1
4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

Guidance literature:: 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid methyl ester; With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 65 ℃; for 96h;

With sodium hydroxide;

With hydrogenchloride; In water; pH=1;

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 1204336-23-1
4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

: 1204336-64-0
[2-(4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoylamino)ethyl]carbamic acid tert-butyl ester

Guidance literature:: 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; N,N-dimethyl-formamide; for 0.25h;

N-BOC-1,2-diaminoethane; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 96h;

Reference yield:

: 1204336-23-1
4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid

: 141-43-5
ethanolamine

: 1204334-73-5
4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-N-(2-hydroxyethyl)-2-methylbenzamide

Guidance literature:: 4-{3-[1-(5-chloropyrimidin-2-yl)piperidin-4-yl]propoxy}-2-methylbenzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; for 0.333333h;

ethanolamine; In tetrahydrofuran; at 40 ℃; for 16h;