Technology Process of C20H17N3OS
There total 7 articles about C20H17N3OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 20 °C
2.1: benzoyl isocyanate / dichloromethane / 0.5 h / Reflux
2.2: 2 h / Reflux
3.1: pyridine / 1 h / 20 °C
With
pyridine; 3-chloro-benzenecarboperoxoic acid; benzoyl isocyanate;
In
dichloromethane; chloroform;
DOI:10.1039/c2ob26705e
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: acetic anhydride; sodium acetate / 0.25 h / Reflux
2.1: hydrogen; platinum on carbon / N,N-dimethyl-formamide / 3.5 h / 3102.97 Torr
3.1: triethylamine / N,N-dimethyl-formamide; dichloromethane / 0 °C
4.1: pyridine; tetraphosphorus decasulfide / 2 h / Reflux
5.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 18 h / 20 °C
6.1: benzoyl isocyanate / dichloromethane / 0.5 h / Reflux
6.2: 2 h / Reflux
7.1: pyridine / 1 h / 20 °C
With
pyridine; tetraphosphorus decasulfide; platinum on carbon; hydrogen; sodium acetate; acetic anhydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; benzoyl isocyanate;
In
dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26705e