C₂₁H₃₀O₇

Base Information

• Chemical Name: C₂₁H₃₀O₇
• CAS No.: 124538-18-7
• Molecular Formula: C₂₁H₃₀O₇
• Molecular Weight: 394.465
• Mol file: 124538-18-7.mol

Synonyms:C₂₁H₃₀O₇

Chemical Property of C₂₁H₃₀O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₃₀O₇

There total 4 articles about C₂₁H₃₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-1-O-methoxymethyl-myo-inositol (124516-79-6) → C21H30O7 (124538-18-7)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1248/cpb.37.791

Reference yield:

benzyl bromide (100-39-0) → C21H30O7 (124538-18-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) 50percent NaH, 2.) 1N KOH / 1.) DMF, mineral oil, 0 deg C, 30 min then R_.T_., 2 h, 2.) MeOH, R_.T_., 2 h

2: 89 percent / 50percent NaH / dimethylformamide; paraffin / 0 deg C, 30 min then R_.T_., 3 h

3: 92 percent / 1percent trifluoroacetic acid / CH₂Cl₂ / 0.5 h / Ambient temperature

With potassium hydroxide; sodium hydride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; paraffin;

DOI:10.1248/cpb.37.791

Reference yield:

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol (124516-77-4) → C21H30O7 (124538-18-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 89 percent / 50percent NaH / dimethylformamide; paraffin / 0 deg C, 30 min then R_.T_., 3 h

2: 92 percent / 1percent trifluoroacetic acid / CH₂Cl₂ / 0.5 h / Ambient temperature

With sodium hydride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; paraffin;

DOI:10.1248/cpb.37.791

upstream raw materials:

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-1-O-methoxymethyl-myo-inositol

benzyl bromide

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

(+/-)-1-O-benzoyl-2,3-O-cyclohexylidene-4,5-O-isopropylidene-myo-inositol

Downstream raw materials:

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-1,5-di-O-methoxymethyl-myo-inositol

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-1,4,5-tri-O-methoxymethyl-myo-inositol

(+/-)-6-O-benzyl-2,3-O-cyclohexylidene-1,4-di-O-methoxymethyl-myo-inositol

C₃₄H₄₈O₁₅