2-Propanone, 1,1-diethoxy-3-phenyl-

Base Information

• Chemical Name: 2-Propanone, 1,1-diethoxy-3-phenyl-
• CAS No.: 19256-31-6
• Molecular Formula: C13H18 O3
• Molecular Weight: 222.284
• European Community (EC) Number: 242-922-8
• DSSTox Substance ID: DTXSID3066473
• Nikkaji Number: J242.755I
• Wikidata: Q81993052
• Mol file: 19256-31-6.mol

Synonyms:1,1-diethoxy-3-phenylpropan-2-one;19256-31-6;2-Propanone, 1,1-diethoxy-3-phenyl-;1,1-Diethoxy-3-phenylacetone;EINECS 242-922-8;2-Propanone,1,1-diethoxy-3-phenyl-;SCHEMBL934793;DTXSID3066473;AKOS015891490;CS-15758;1,1-DIETHOXY-3-PHENYL-2-PROPANONE;CS-0043260;FT-0723653;Pyruvaldehyde, phenyl-, 1-(diethyl acetal);A51235

Chemical Property of 2-Propanone, 1,1-diethoxy-3-phenyl-

Chemical Property:

• Vapor Pressure: 0.000188mmHg at 25°C
• Boiling Point: 328.6°Cat760mmHg
• Flash Point: 143.6°C
• Density: 1.033g/cm³
• Storage Temp.: 2-8°C
• XLogP3: 2.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 7
• Exact Mass: 222.125594432
• Heavy Atom Count: 16
• Complexity: 191

Purity/Quality:

97% ^*data from raw suppliers

1,1-Diethoxy-3-phenylpropan-2-one 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(C(=O)CC1=CC=CC=C1)OCC

Technology Process of 2-Propanone, 1,1-diethoxy-3-phenyl-

There total 8 articles about 2-Propanone, 1,1-diethoxy-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C16H14BF2NO + ethanol (64-17-5) → 1,1-diethoxy-3-phenylpropane-2-one (19256-31-6)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1021/jo0711034

Reference yield: 96.0%

benzylmagnesium chloride (6921-34-2) + Ethyl diethoxyacetate (6065-82-3) → 1,1-diethoxy-3-phenylpropane-2-one (19256-31-6)

Guidance literature:

In tetrahydrofuran; at -78 ℃; for 2h;

DOI:10.1081/SCC-120013744

Reference yield:

Ethylethoxy diacetate + benzylmagnesium chloride (6921-34-2) → 1,1-diethoxy-3-phenylpropane-2-one (19256-31-6)

Guidance literature:

With ammonium chloride; In tetrahydrofuran; hexane; ethyl acetate;

upstream raw materials:

ethanol

benzylglyoxal

benzylmagnesium chloride

Ethyl diethoxyacetate

Downstream raw materials:

2-benzyl-8-benzyl-6-(phenyl)imidazo[1,2-a]pyrazin-3(7H)-one

(S)-N-(1-oxo-3-phenylpropan-2-yl)benzamide

N-benzoyl-L-phenylalanine

L-phenylalanine hydrochloride