methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate

Base Information

Chemical Name:methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate
CAS No.:850832-50-7
Molecular Formula:C₁₅H₁₂BrNO₂
Molecular Weight:318.17
Hs Code.:

Synonyms:methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate

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Technology Process of methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate

There total 1 articles about methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 67-56-1
methanol

: 5847-76-7
(2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylic acid

: 850832-50-7
methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate

Guidance literature:: methanol; With thionyl chloride; at -10 ℃; for 0.333333h;

(2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylic acid; at -10 - 70 ℃; for 14h;

Reference yield:

: 850832-50-7
methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 850832-51-8
(3E)-3-(4-bromophenyl)-1,1,1-trifluoro-4-pyridin-3-ylbut-3-en-2-one

Guidance literature:: methyl (2E)-2-(4-bromophenyl)-3-pyridin-3-ylacrylate; (trifluoromethyl)trimethylsilane; With cesium fluoride; In 1,2-dimethoxyethane; at 20 ℃; for 1h;

With hydrogenchloride; In 1,2-dimethoxyethane; water; at 20 ℃; for 3h;