5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

Base Information

Chemical Name:5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride
CAS No.:1027294-29-6
Molecular Formula:C₂₃H₃₀ClN₃O₂
Molecular Weight:415.963
Hs Code.:

Synonyms:5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

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Technology Process of 5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

There total 4 articles about 5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137292-30-9
(+/-)-(E)-5-[2-benzyl-2-(imidazol-1-yl)-1-cyclohexylethylidene]aminooxypentanoic acid

: 1027294-29-6
5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

Guidance literature:: With thionyl chloride; In chloroform; for 2h; Ambient temperature;
DOI:10.1021/jm00047a016

Reference yield:

: 14660-52-7
ethyl 5-bromovalerate

: 1027294-29-6
5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, RT, 2.) DMF, RT, 2 h

2: 60 percent / 1N aq. NaOH / ethanol / 4 h / Ambient temperature

3: SOCl₂ / CHCl₃ / 2 h / Ambient temperature

With sodium hydroxide; thionyl chloride; sodium hydride; In ethanol; chloroform;
DOI:10.1021/jm00047a016

Reference yield:

: (+/-)-(E+Z)-1-cyclohexyl-2-(1H-imidazol-1-yl)-3-phenylpropan-1-one oxime

: 1027294-29-6
5-[1-Cyclohexyl-2-imidazol-1-yl-3-phenyl-prop-(E)-ylideneaminooxy]-pentanoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, RT, 2.) DMF, RT, 2 h

2: 60 percent / 1N aq. NaOH / ethanol / 4 h / Ambient temperature

3: SOCl₂ / CHCl₃ / 2 h / Ambient temperature

With sodium hydroxide; thionyl chloride; sodium hydride; In ethanol; chloroform;
DOI:10.1021/jm00047a016