anthranilic acid-(2,2,2-trifluoro-ethyl ester)

Base Information

Chemical Name:anthranilic acid-(2,2,2-trifluoro-ethyl ester)
CAS No.:653-96-3
Molecular Formula:C₉H₈F₃NO₂
Molecular Weight:219.163
Hs Code.:

Synonyms:anthranilic acid-(2,2,2-trifluoro-ethyl ester)

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Chemical Property of anthranilic acid-(2,2,2-trifluoro-ethyl ester)

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Technology Process of anthranilic acid-(2,2,2-trifluoro-ethyl ester)

There total 4 articles about anthranilic acid-(2,2,2-trifluoro-ethyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86451-26-5
2,2'-(phenyl-λ³-iodanediyl)bis(isoindoline-1,3-dione)

: 1356116-56-7
2,2,2-trifluoroethyl 2-(((2,2,2-trifluoroethoxy)carbonyl)amino)benzoate

: 653-96-3
anthranilic acid-(2,2,2-trifluoro-ethyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1.1: [hydroxy(tosyloxy)iodo]benzene; potassium carbonate; sodium sulfate / acetonitrile / 6 h / 20 °C

2.1: iodobenzene; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid / 0.17 h / 0 °C / Inert atmosphere

2.2: 8 h / 0 - 40 °C / Inert atmosphere

With iodobenzene; [hydroxy(tosyloxy)iodo]benzene; potassium carbonate; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid; In acetonitrile; 1.1: Hofmann-type rearrangement / 2.2: Hofmann-type rearrangement;
DOI:10.1021/ol300028j

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 75-89-8
2,2,2-trifluoroethanol

: 1356116-56-7
2,2,2-trifluoroethyl 2-(((2,2,2-trifluoroethoxy)carbonyl)amino)benzoate

: 653-96-3
anthranilic acid-(2,2,2-trifluoro-ethyl ester)

Guidance literature:: 2,2,2-trifluoroethanol; With iodobenzene; toluene-4-sulfonic acid; sodium sulfate; 3-chloro-benzenecarboperoxoic acid; at 0 ℃; for 0.166667h; Inert atmosphere;

phthalimide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 0 - 40 ℃; for 8h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol300028j