C₂₂H₂₀FNO₅S

Base Information

Chemical Name:C₂₂H₂₀FNO₅S
CAS No.:1374232-97-9
Molecular Formula:C₂₂H₂₀FNO₅S
Molecular Weight:429.469
Hs Code.:

C<sub>22</sub>H<sub>20</sub>FNO<sub>5</sub>S

Synonyms:C₂₂H₂₀FNO₅S

Suppliers and Price of C₂₂H₂₀FNO₅S

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Chemical Property of C₂₂H₂₀FNO₅S

Chemical Property:

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Technology Process of C₂₂H₂₀FNO₅S

There total 11 articles about C₂₂H₂₀FNO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 1374232-96-8
C₂₀H₁₈FNO₃S

: 1374232-97-9
C₂₂H₂₀FNO₅S

Guidance literature:: With sodium acetate; potassium carbonate; copper dichloride; palladium dichloride; at 20 ℃;

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 1374232-97-9
C₂₂H₂₀FNO₅S

Guidance literature:: Multi-step reaction with 11 steps

1.1: copper(l) iodide; copper diacetate / water / 48 h / 100 °C

2.1: polyphosphoric acid / 3 h / 90 °C

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C

4.2: 0 - 20 °C

5.1: diethylzinc / hexane; toluene / 0 - 20 °C

6.1: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

7.1: boron tribromide / dichloromethane / 1 h / -20 - 0 °C

7.2: Cooling with ice

8.1: triethylamine / dmap / tetrahydrofuran / 10 h / 0 - 20 °C

9.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

10.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

11.1: sodium acetate; potassium carbonate / copper dichloride; palladium dichloride / 20 °C

With piperidine; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; diethylzinc; sodium acetate; boron tribromide; potassium carbonate; triethylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; copper diacetate; copper dichloride; palladium dichloride; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 879-56-1
7-Methoxy-2,3-dihydro-1H-quinolin-4-one

: 1374232-97-9
C₂₂H₂₀FNO₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / 0 °C

2.2: 0 - 20 °C

3.1: diethylzinc / hexane; toluene / 0 - 20 °C

4.1: N-Bromosuccinimide / dichloromethane / 1 h / 0 - 20 °C

5.1: boron tribromide / dichloromethane / 1 h / -20 - 0 °C

5.2: Cooling with ice

6.1: triethylamine / dmap / tetrahydrofuran / 10 h / 0 - 20 °C

7.1: piperidine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

8.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C

9.1: sodium acetate; potassium carbonate / copper dichloride; palladium dichloride / 20 °C

With piperidine; hydrogenchloride; N-Bromosuccinimide; n-butyllithium; diethylzinc; sodium acetate; boron tribromide; potassium carbonate; triethylamine; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tri-tert-butyl phosphine; copper dichloride; palladium dichloride; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;