6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

Base Information

Chemical Name:6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane
CAS No.:15223-09-3
Molecular Formula:C₃₄H₅₄O₄S
Molecular Weight:558.866
Hs Code.:

Synonyms:6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

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Technology Process of 6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

There total 10 articles about 6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 570-85-4
5α-cholestane-3β,6β-diol

: 98-59-9
p-toluenesulfonyl chloride

: 15223-09-3
6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

Guidance literature:: In pyridine; Ambient temperature;
DOI:10.1248/cpb.35.986

Reference yield:

: 57-88-5
cholesterol

: 15223-09-3
6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

Guidance literature:: Multi-step reaction with 5 steps

2: 75 percent / 6 M hydrochloric acid / tetrahydrofuran / 1 h / Ambient temperature

3: 82 percent / pyridine / Ambient temperature

4: 75 percent / lithium aluminum hydride / tetrahydrofuran / 1 h / Ambient temperature

5: 91 percent / pyridine / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; pyridine;
DOI:10.1248/cpb.35.986

Reference yield:

: 1256-83-3
Acetic acid (3S,5S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-6-oxo-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

: 15223-09-3
6β-hydroxy-3β-p-toluenesulfonyloxy-5α-cholestane

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / lithium aluminum hydride / tetrahydrofuran / 1 h / Ambient temperature

2: 91 percent / pyridine / Ambient temperature

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine;
DOI:10.1248/cpb.35.986