2-(Tetrahydro-2-thienyl)pyridine

Base Information

Chemical Name:2-(Tetrahydro-2-thienyl)pyridine
CAS No.:76732-76-8
Molecular Formula:C9H11 N S
Molecular Weight:165.259
Hs Code.:2934999090
European Community (EC) Number:278-533-5
DSSTox Substance ID:DTXSID90998048
Nikkaji Number:J309.316F
Mol file:76732-76-8.mol

Synonyms:76732-76-8;2-(Tetrahydro-2-thienyl)pyridine;EINECS 278-533-5;2-(thiolan-2-yl)pyridine;tetrahydrothienylpyridine;SCHEMBL9422116;DTXSID90998048;MCXIBJPBLIURRN-UHFFFAOYSA-N;2-(pyrid-2-yl)tetrahydrothiophene;2-(Pyrid-2-yl)-tetrahydrothiophene;AKOS006372514;2-[(Tetrahydrothiophen)-2-yl]pyridine

Suppliers and Price of 2-(Tetrahydro-2-thienyl)pyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-(Tetrahydro-2-thienyl)pyridine

Chemical Property:

Vapor Pressure:0.00239mmHg at 25°C
Boiling Point:297.4°C at 760 mmHg
Flash Point:133.7°C
PSA：38.19000
Density:1.135g/cm³
LogP:2.64970
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:165.06122053
Heavy Atom Count:11
Complexity:127

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(SC1)C2=CC=CC=N2

Technology Process of 2-(Tetrahydro-2-thienyl)pyridine

There total 6 articles about 2-(Tetrahydro-2-thienyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76732-77-9
3-chloropropyl 2-pyridylmethyl sulfide

: 76732-76-8
2-(2-pyridyl)tetrahydrothiophene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 1h; Ambient temperature;
DOI:10.1021/jm00384a004

Reference yield:

: 680-31-9
N,N,N,N,N,N-hexamethylphosphoric triamide

: 865-47-4
potassium tert-butylate

: 76732-77-9
3-chloropropyl 2-pyridylmethyl sulfide

: 76732-76-8
2-(2-pyridyl)tetrahydrothiophene

Guidance literature:: In tetrahydrofuran; diethyl ether; water;

Reference yield:

: 2044-73-7
2-(sulfanylmethyl)pyridine

: 76732-76-8
2-(2-pyridyl)tetrahydrothiophene

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH

2: 70 percent / t-BuOK / tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / Ambient temperature

With sodium hydroxide; potassium tert-butylate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1021/jm00384a004