[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

Base Information

Chemical Name:[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]
CAS No.:891864-95-2
Molecular Formula:C₂₄H₂₇ClNO₃PPd
Molecular Weight:550.33
Hs Code.:

Synonyms:[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

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Chemical Property of [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

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Technology Process of [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

There total 2 articles about [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 110-63-4
Butane-1,4-diol

: 53080-45-8
dichloro[2-(β-diphenylphosphinoethyl)pyridine]palladium(II)

: 201230-82-2
carbon monoxide

: 891864-95-2
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

Guidance literature:: With N(C₂H₅)3; In acetonitrile; byproducts: triethylammonium chloride; charging of 1,4-dihydroxybutane, NEt3, PdCl2(PPh2CH2CH2C5H4N) and CH3CN in glass reactor; treatment with CO under stirring at atmospheric pressure and room temp. for 3 h; concn., addn. of Et2O; treatment with CO for 48 h; cooling at -10°C overnight; crystn., filtration, washing, addn. of Et2O; cooling at -10°C for 5 ds; crystn., washing with mixt. ofEt2O-CH3CN (4:1); drying; elem. anal.;
DOI:10.1021/om060012e

Reference yield:

: 891864-86-1
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

: 891864-95-2
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile; methanol

2: N(C₂H₅)3 / acetonitrile

With N(C₂H₅)3; In methanol; acetonitrile;
DOI:10.1021/om060012e

Reference yield:

: 891864-95-2
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2CH2CH2OH)]

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile; methanol

2: N(C₂H₅)3 / acetonitrile

3: N(C₂H₅)3 / acetonitrile

With N(C₂H₅)3; In methanol; acetonitrile;
DOI:10.1021/om060012e