[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

Base Information

Chemical Name:[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]
CAS No.:891864-86-1
Molecular Formula:C₂₂H₂₃ClNO₃PPd
Molecular Weight:522.276
Hs Code.:

Synonyms:[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

Suppliers and Price of [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

There total 1 articles about [PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 53080-45-8
dichloro[2-(β-diphenylphosphinoethyl)pyridine]palladium(II)

: 201230-82-2
carbon monoxide

: 107-21-1
ethylene glycol

: 891864-86-1
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

Guidance literature:: With N(C₂H₅)3; In acetonitrile; byproducts: triethylammonium chloride; addn. of 1,2-didroxyethane and NEt3 to suspn. of PdCl2(PPh2CH2CH2C5H4N) in CH3CN; pumping off N2; admitting of CO (0.1 Mpa); stirring at room temp. for 4 h; concn., addn. of Et2O; treatment with CO for 12 h at room temp.; filtration, washing twice with cold mixt. of Et2O-CH3CN (4:1); drying invac.; cooling of mother liquor overnight at -10°C; dissolving of NEt3*HCl with Et2O-CH3CN, elem. anal.;
DOI:10.1021/om060012e

Reference yield:

: 891864-86-1
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

: 7440-05-3
palladium

Guidance literature:: In acetonitrile; byproducts: HCl, 2-(β-diphenylphosphine)ethylpyridine, 1,3-dioxolan-2-one; (N2); heating at T > 40°C in CH3CN;
DOI:10.1021/om060012e

Reference yield:

: 891864-86-1
[PdCl(2-(β-diphenylphosphine)ethylpyridine)(COOCH2CH2OH)]

: 603-35-0
triphenylphosphine

: 14221-01-3
tetrakis(triphenylphosphine) palladium⁽⁰⁾

Guidance literature:: With N(C₂H₅)3; In acetonitrile; byproducts: N(C2H5)3*HCl, 1,3-dioxolan-2-one, 2-(β-diphenylphosphine)ethylpyridine; (N2); addn. of PPh3 (excess) and NEt3 to suspn. of PdCl(PPh2CH2CH2C5H4N)(COOCH2CH2OH) in CH3CN; heating at 60°C for 3 h; pptn.;
DOI:10.1021/om060012e