Technology Process of C37H36ClN5O5
There total 10 articles about C37H36ClN5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: thionyl chloride / N,N-dimethyl-formamide / 17 h / 20 °C / Heating / reflux
2: triethylamine / N,N-dimethyl-formamide / isopropyl alcohol / 17 h / 20 °C
3: methanol / 16 h / Heating / reflux
4: lithium chloride / N,N-dimethyl-formamide / 5 h / 150 °C
5: potassium carbonate / acetone / 6 h / 80 °C
6: xylene / 2 h / 150 °C
7: potassium carbonate / acetone / 5 h / 20 °C / Heating / reflux
8: hydrogen; potassium carbonate / platinum(IV) oxide / methanol / 2 h / 20 °C
9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C
With
dmap; thionyl chloride; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; lithium chloride;
platinum(IV) oxide; N,N-dimethyl-formamide;
In
methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; acetone; xylene;
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: xylene / 2 h / 150 °C
2: potassium carbonate / acetone / 5 h / 20 °C / Heating / reflux
3: hydrogen; potassium carbonate / platinum(IV) oxide / methanol / 2 h / 20 °C
4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C
With
dmap; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
platinum(IV) oxide;
In
methanol; dichloromethane; acetone; xylene;