2-Acetamido-1-Nitronaphthalene

Base Information

• Chemical Name: 2-Acetamido-1-Nitronaphthalene
• CAS No.: 5419-82-9
• Molecular Formula: C12H10N2O3
• Molecular Weight: 230.223
• Mol file: 5419-82-9.mol

Synonyms:2-Acetamido-1-nitronaphthalene;

Chemical Property of 2-Acetamido-1-Nitronaphthalene

Chemical Property:

• Vapor Pressure: 3.73E-09mmHg at 25°C
• Refractive Index: 1.697
• Boiling Point: 474.1 °C at 760 mmHg
• Flash Point: 240.5 °C
• PSA: 74.92000
• Density: 1.366 g/cm³
• LogP: 3.30260
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

N-(1-Nitronaphthalen-2-yl)acetamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Acetamido-1-Nitronaphthalene

There total 9 articles about 2-Acetamido-1-Nitronaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetylaminonaphthalene (581-97-5) + nitric acid (7697-37-2,78989-43-2) + acetic acid (64-19-7,77671-22-8) → 2-Acetamido-6-nitro-naphthalin (102877-11-2) + 1-nitro-2-acetylaminonaphthalene (5419-82-9) + N-(8-nitro-[2]naphthyl)-acetamide (102877-13-4)

Guidance literature:

DOI:10.1021/ja01341a029

Reference yield:

2-acetylaminonaphthalene (581-97-5) → 1-nitro-2-acetylaminonaphthalene (5419-82-9) + N-(8-nitro-[2]naphthyl)-acetamide (102877-13-4)

Guidance literature:

With nitric acid; acetic acid; at 30 - 40 ℃; man waescht die ausgeschiedenen Krystalle mit Essigsaeure, kocht sie mit Benzol und filtriert lauwarm;

Reference yield:

2-acetylaminonaphthalene (581-97-5) + nitric acid (7697-37-2,78989-43-2) → 1-nitro-2-acetylaminonaphthalene (5419-82-9) + N-(8-nitro-[2]naphthyl)-acetamide (102877-13-4)

Guidance literature:

upstream raw materials:

2-acetylaminonaphthalene

nitric acid

acetic acid

naphthalen-2-ylamine

Downstream raw materials:

1-nitro-2-naphthol

ammonia

1-nitro-2-naphthylamine

acetic acid