1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine

Base Information

• Chemical Name: 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine
• CAS No.: 169614-08-8
• Molecular Formula: C₁₁H₁₂N₂O₆S
• Molecular Weight: 300.292

Synonyms:1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine

Chemical Property of 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine

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Technology Process of 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine

There total 10 articles about 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.2%

1a,2,6,6a-tetrahydro-1H,4H-<1,3>-dioxepino<5,6-b>azirine (151021-81-7) + 4-Nitrobenzenesulfonyl chloride (98-74-8) → 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine (169614-08-8)

Guidance literature:

With pyridine; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/jm00016a006

Reference yield: 68.0%

1-[(4-nitrophenyl)sulphinyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine → 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine (169614-08-8)

Guidance literature:

With potassium permanganate; acetic acid; In ethyl acetate; at 5 ℃;

Reference yield: 67.0%

1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine (930285-83-9) → 1-[(4-nitrophenyl)sulphinyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine + 1-<(4-nitrophenyl)sulfonyl>-1a,2,6,6a-tetrahydro-1H,4H-<1,3>dioxepino<5,6-b>azirine (169614-08-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

upstream raw materials:

1a,2,6,6a-tetrahydro-1H,4H-<1,3>-dioxepino<5,6-b>azirine

4-Nitrobenzenesulfonyl chloride

1-[(4-nitrophenyl)sulphanyl]-1a,2,6,6a-tetrahydro-1H,4H-[1,3]dioxepino[5,6-b]azirine

4-nitrobenzenesulfenyl chloride

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