ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

Base Information

Chemical Name:ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate
CAS No.:1323921-55-6
Molecular Formula:C₂₁H₂₂N₂O₄
Molecular Weight:366.417
Hs Code.:

Synonyms:ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

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Chemical Property of ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

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Technology Process of ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

There total 3 articles about ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 91-21-4
1,2,3,4-tetrahydroisoquinoline

: 924-44-7
glyoxylic acid ethyl ester

: 5153-67-3
nitrostyrene

: 1323921-55-6
ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

Guidance literature:: With benzoic acid; In toluene; at 80 ℃; for 2.5h;
DOI:10.1021/acs.orglett.7b00769

Reference yield: 49.0%

: 102-96-5
(2-nitroethenyl)benzene

: 88014-09-9
(3,4-dihydro-1H-isoquinolin-2-yl)-acetic acid ethyl ester

: 1323921-55-6
ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

Guidance literature:: With tris(2,2'-bipyridine)ruthenium dichloride; oxygen; In acetonitrile; at 20 ℃; for 10h; Irradiation;
DOI:10.1002/anie.201102306

Reference yield:

: 102-96-5
(2-nitroethenyl)benzene

: 1323921-57-8
C₁₃H₁₆⁽²⁾HNO₂

: 1323921-55-6
ethyl 1-nitro-2-phenyl-1,2,3,5,6,10b-hexahydropyrrolo[2,1-a]isoquinoline-3-carboxylate

: 1323921-59-0
C₂₁H₂₁⁽²⁾HN₂O₄

Guidance literature:: With tris(2,2'-bipyridine)ruthenium dichloride; oxygen; In acetonitrile; at 20 ℃; for 10h; Irradiation;
DOI:10.1002/anie.201102306