2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Base Information

Chemical Name:2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate
CAS No.:129245-42-7
Molecular Formula:C₂₁H₃₈O₅Si₂
Molecular Weight:426.701
Hs Code.:

Synonyms:2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

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Chemical Property of 2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

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Technology Process of 2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

There total 5 articles about 2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 129245-41-6
(1R,2S,4S,5S)-2-Hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylic acid

: 129245-42-7
2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1039/a605894i

Reference yield:

: 129245-40-5
Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

: 129245-42-7
2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / aq. NaOH / ethanol / 48 h / 5 °C

2: 82 percent / DMAP, DCC / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1039/a605894i

Reference yield:

: 129312-19-2
Ethyl (1R,2S,4S,5S)-2,4-dihydroxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

: 129245-42-7
2-Trimethylsilylethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Ag₂O / 48 h / Heating

2: 99 percent / aq. NaOH / ethanol / 48 h / 5 °C

3: 82 percent / DMAP, DCC / CH₂Cl₂ / 16 h / Ambient temperature

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; silver(l) oxide; In ethanol; dichloromethane;
DOI:10.1039/a605894i