Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Base Information

Chemical Name:Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate
CAS No.:129245-40-5
Molecular Formula:C₁₈H₃₀O₅Si
Molecular Weight:354.519
Hs Code.:

Synonyms:Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

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Chemical Property of Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

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Technology Process of Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

There total 3 articles about Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 129312-19-2
Ethyl (1R,2S,4S,5S)-2,4-dihydroxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

: 74-88-4
methyl iodide

: 129245-40-5
Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Guidance literature:: With silver(l) oxide; for 48h; Heating;
DOI:10.1039/a605894i

Reference yield:

: 129313-41-3
Ethyl (1R,2S,4S,5S)-2-hydroxy-4-<(2S)-2-hydroxy-2-phenylacetoxy>-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

: 129245-40-5
Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / K₂CO₃ / ethanol / 16 h / Ambient temperature

2: 100 percent / Ag₂O / 48 h / Heating

With potassium carbonate; silver(l) oxide; In ethanol;
DOI:10.1039/a605894i

Reference yield:

: (1RS,2SR,5SR)-ethyl 2-hydroxy-5-methyl-4-oxo-2-(2'-trimethylsilyl-3'-furyl)cyclohexanecarboxylate

: 129245-40-5
Ethyl (1R,2S,4S,5S)-2-hydroxy-4-methoxy-5-methyl-2-(2-trimethylsilyl-3-furyl)cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH(OAc)3 / acetic acid

2: Ag₂O / 48 h / Heating

With sodium tris(acetoxy)borohydride; silver(l) oxide; In acetic acid;
DOI:10.1039/c39890001250