bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide

Base Information

Chemical Name:bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide
CAS No.:464884-88-6
Molecular Formula:Br*C₅₂H₆₀NO₁₂
Molecular Weight:970.952
Hs Code.:

Synonyms:bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide

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Chemical Property of bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide

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Technology Process of bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide

There total 1 articles about bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 124-40-3
dimethyl amine

: 176650-93-4
3,5-bis(3,5-dimethoxybenzocarboxymethyl)benzyl bromide

: 464884-88-6
bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide

Guidance literature:: With sodium carbonate; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1021/ja017613b

Reference yield:

: 11Na⁽¹⁺⁾*NH₄⁽¹⁺⁾*(Mn(H₂O))3(SbW₉O₃₃)2^(12-)*45H₂O=Na₁₁(NH₄)((Mn(H₂O))3(SbW₉O₃₃)2)*45H₂O

: 464884-88-6
bis-{3,5-bis[3,5-(dimethoxy)benzyloxy]benzyl}-dimethylammonium bromide

: 12(CH₃)2N(CH₂C₆H₃(OCH₂C₆H₃(OCH₃)2)2)2⁽¹⁺⁾*(Mn(H₂O))3(SbW₉O₃₃)2^(12-)*15H₂O=(C₅₂H₆₀NO₁₂)12((Mn(H₂O))3(SbW₉O₃₃)2)*15H₂O

Guidance literature:: In chloroform; water; Sb-W compd. dissolved in water; bromide (12 equiv.) in CHCl3 added; transferred into org. phase by gentle shaking of biphasic soln.; org. phase sepd.; evapd.; dried at 3 mbar (20°C) for 3 d; elem. anal.;
DOI:10.1021/ja017613b