C₃₈H₅₀O₆Si

Base Information

Chemical Name:C₃₈H₅₀O₆Si
CAS No.:935248-52-5
Molecular Formula:C₃₈H₅₀O₆Si
Molecular Weight:630.897
Hs Code.:

C<sub>38</sub>H<sub>50</sub>O<sub>6</sub>Si

Synonyms:C₃₈H₅₀O₆Si

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Chemical Property of C₃₈H₅₀O₆Si

Chemical Property:

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Technology Process of C₃₈H₅₀O₆Si

There total 10 articles about C₃₈H₅₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 935248-47-8
9-(tert-butyl-dimethyl-silanyloxy)-3,5-dihydroxy-7-(4-methoxy-benzyloxy)-8,8-dimethyl-nonanoic acid methyl ester

: 935248-52-5
C₃₈H₅₀O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / Otera's catalyst / hexane / 3 h / Heating

2: imidazole / dimethylformamide / 3 h / 50 °C

3: 3.4 g / AcOH / H₂O / 11 h / 20 °C

4: NaHCO₃; Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / 20 °C

5: 1.42 g / In / dimethylformamide / 16 h / 20 °C

With 1H-imidazole; indium; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; Otera's catalyst; In hexane; dichloromethane; water; N,N-dimethyl-formamide; 4: Dess-Martin oxidation;
DOI:10.1021/ja067305j

Reference yield:

: 935248-51-4
C₃₅H₄₄O₆Si

: 556-56-9
allyl iodid

: 935248-52-5
C₃₈H₅₀O₆Si

Guidance literature:: With indium; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/ja067305j

Reference yield:

: 935248-44-5
5-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-4,4-dimethyl-pentan-1-ol

: 935248-52-5
C₃₈H₅₀O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: aq. NaOCl; NaHCO₃ / KBr; TEMPO / CH₂Cl₂ / 0.5 h

2.1: Ti(Oi-Pr)4; TiCl₄ / toluene / 0.33 h / -78 °C

2.2: 9.77 g / toluene / 0.5 h / -78 °C

3.1: 91 percent / (CH₃)4NBH(OAc)3; AcOH / acetonitrile / 40 h / -35 °C

4.1: 86 percent / Otera's catalyst / hexane / 3 h / Heating

5.1: imidazole / dimethylformamide / 3 h / 50 °C

6.1: 3.4 g / AcOH / H₂O / 11 h / 20 °C

7.1: NaHCO₃; Dess-Martin periodinane / CH₂Cl₂ / 1.5 h / 20 °C

8.1: 1.42 g / In / dimethylformamide / 16 h / 20 °C

With 1H-imidazole; titanium(IV) isopropylate; indium; sodium hypochlorite; titanium tetrachloride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 2,2,6,6-tetramethyl-piperidine-N-oxyl; Otera's catalyst; potassium bromide; In hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 7.1: Dess-Martin oxidation;
DOI:10.1021/ja067305j