Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester
CAS No.:50850-20-9
Molecular Formula:C₁₅H₁₇N₃O₂
Molecular Weight:271.319
Hs Code.:
DSSTox Substance ID:DTXSID401153545

Synonyms:DTXSID401153545;Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester;50850-20-9

Suppliers and Price of Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:271.132076794
Heavy Atom Count:20
Complexity:318

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=NC(=C1NC(=O)OCC2=CC=CC=C2)N)C

Technology Process of Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester

There total 5 articles about Carbamic acid, (2-amino-4,6-dimethyl-3-pyridinyl)-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 50850-16-3
2,3-diamino-4,6-dimethylpyridine

: 501-53-1,94274-21-2
benzyl chloroformate

: 50850-20-9
N³-benzyloxycarbonyl-2,3-diamino-4,6-dimethylpyridine

: (3-benzyloxycarbonylamino-4,6-dimethyl-pyridin-2-yl)-carbamic acid benzyl ester

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 18h;
DOI:10.1002/jhet.5570400403

Reference yield:

: 89856-44-0
2-amino-5-bromo-4,6-dimethylpyridine

: 50850-20-9
N³-benzyloxycarbonyl-2,3-diamino-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / potassium nitrate; concd. sulfuric acid / 1 h / 20 °C

2: 98 percent / hydrogen; ammonium hydroxide / palladium on carbon / methanol / 18 h / 50 °C / 2585.74 Torr

3: 49 percent / potassium carbonate / acetone / 18 h / 20 °C

With ammonium hydroxide; sulfuric acid; hydrogen; potassium carbonate; potassium nitrate; palladium on activated charcoal; In methanol; acetone;
DOI:10.1002/jhet.5570400403

Reference yield:

: 89791-76-4
2-amino-3-nitro-4,6-dimethyl-5-bromo-pyridine

: 50850-20-9
N³-benzyloxycarbonyl-2,3-diamino-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / hydrogen; ammonium hydroxide / palladium on carbon / methanol / 18 h / 50 °C / 2585.74 Torr

2: 49 percent / potassium carbonate / acetone / 18 h / 20 °C

With ammonium hydroxide; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; acetone;
DOI:10.1002/jhet.5570400403