tetracyclohexyldiborane⁽⁶⁾

Base Information

• Chemical Name: tetracyclohexyldiborane⁽⁶⁾
• CAS No.: 54765-85-4
• Molecular Formula: C₂₄H₄₆B₂
• Molecular Weight: 356.251
• Mol file: 54765-85-4.mol

Synonyms:tetracyclohexyldiborane⁽⁶⁾

Chemical Property of tetracyclohexyldiborane⁽⁶⁾

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetracyclohexyldiborane⁽⁶⁾

There total 6 articles about tetracyclohexyldiborane⁽⁶⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(cyclo-C6H11)2B(O-C6H4-2-CH3) (32705-38-7) → tetracyclohexyldiborane(6) (54765-85-4)

Guidance literature:

With lithium aluminium tetrahydride; In hexane;

DOI:10.1016/S0022-328X(00)80144-8

Reference yield:

diborane (19287-45-7) + cyclohexene (110-83-8) → tetracyclohexyldiborane(6) (54765-85-4)

Guidance literature:

In diethylene glycol; at 0°C;;

DOI:10.1021/ja00867a024 DOI:10.1021/ja00897a010

Reference yield:

B-methoxydicyclohexylborane (32705-46-7) → tetracyclohexyldiborane(6) (54765-85-4)

Guidance literature:

With lithium aluminium tetrahydride; trapping with isobutylene;;

DOI:10.1021/ja00725a050

upstream raw materials:

diborane

cyclohexene

dimethyl sulfide borane

sodium tetrahydroborate

Downstream raw materials:

boric acid

[(1,2-bis(dimethylphosphino)ethane)NiMe(Ph₂PCH₂CH₂BCy₂)][MeB(C₆F₅)3]

(1,2-bis(dimethylphosphino)ethane)NiMe(Ph₂PCH₂CH₂BCy₂Me)

B(cyclohexyl)2(OC₆H₄CHNC₆H₄OMe)