4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

Base Information

Chemical Name:4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol
CAS No.:1312788-48-9
Molecular Formula:C₃₀H₃₈BNO₅
Molecular Weight:503.446
Hs Code.:

Synonyms:4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

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Chemical Property of 4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

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Technology Process of 4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

There total 8 articles about 4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955931-17-6
(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

: 1192765-29-9
4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenol

: 1312788-48-9
4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

Guidance literature:: With tributylphosphine; diamide; In tetrahydrofuran; at 20 ℃; for 2h; cooling with ice;

Reference yield:

: 83647-43-2
3-bromo-2-methylbenzyl alcohol

: 1312788-48-9
4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium p-toluenesulfonate / dichloromethane / 1.5 h / 20 °C

2.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 1 h / Inert atmosphere; Reflux

3.1: potassium phosphate / dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate / water; toluene / 0.5 h / Reflux

3.2: 2 h / Reflux

4.1: tributylphosphine / diamide / tetrahydrofuran / 2 h / 20 °C / cooling with ice

With potassium phosphate; tributylphosphine; potassium acetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diamide; palladium diacetate; pyridinium p-toluenesulfonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene;

Reference yield:

: 17689-66-6
3-hydroxy-3-methylbutyl toluene-4-sulfonate

: 1312788-48-9
4-(5-(3-((4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)methyl)-2-methylphenyl)-4-methylpyridin-2-yloxy)-2-methylbutan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / cooling with ice

1.2: 4 h / 60 °C

2.1: potassium phosphate / dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate / water; toluene / 0.5 h / Reflux

2.2: 2 h / Reflux

3.1: tributylphosphine / diamide / tetrahydrofuran / 2 h / 20 °C / cooling with ice

With potassium phosphate; tributylphosphine; sodium hydride; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; diamide; palladium diacetate; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; mineral oil;