(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

Base Information

Chemical Name:(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol
CAS No.:955931-17-6
Molecular Formula:C₁₉H₂₅NO₃
Molecular Weight:315.412
Hs Code.:

Synonyms:(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

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Chemical Property of (3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

Chemical Property:

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Technology Process of (3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

There total 6 articles about (3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955930-01-5
4-[(5-bromo-4-methylpyridin-2-yl)oxy]2-methylbutan-2-ol

: 1294453-67-0
5,5-dimethyl-2-(2-methyl-3-((tetrahydro-2H-pyran-2-yloxy)methyl)phenyl)-1,3,2-dioxaborinane

: 955931-17-6
(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

Guidance literature:: 4-[(5-bromo-4-methylpyridin-2-yl)oxy]2-methylbutan-2-ol; 5,5-dimethyl-2-(2-methyl-3-((tetrahydro-2H-pyran-2-yloxy)methyl)phenyl)-1,3,2-dioxaborinane; With potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In water; toluene; for 0.5h; Reflux;

With water; acetic acid; In toluene; for 2h; Reflux;

Reference yield:

: 134638-86-1
2-((3-bromo-2-methylphenyl)methoxy)tetrahydro-2H-pyran

: 955931-17-6
(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 1 h / Reflux

2.1: potassium phosphate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene; water / 0.5 h / Reflux

2.2: 2 h / Reflux

With potassium phosphate; potassium acetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium diacetate; In 1,4-dioxane; water; toluene;

Reference yield:

: 164513-38-6
2-hydroxy-5-bromo-4-methylpyridine

: 955931-17-6
(3-(6-(3-hydroxy-3-methylbutoxy)-4-methylpyridin-3-yl)-2-methylphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Cooling with ice

1.2: 4 h / 60 °C

2.1: potassium phosphate / palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene; water / 0.5 h / Reflux

2.2: 2 h / Reflux

With potassium phosphate; sodium hydride; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In water; N,N-dimethyl-formamide; toluene; mineral oil;