tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

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Chemical Name:tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate
CAS No.:1258946-46-1
Molecular Formula:C₂₃H₃₅N₂O₆*ClO₄
Molecular Weight:534.991
Hs Code.:

Synonyms:tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

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Chemical Property of tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

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Technology Process of tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

There total 3 articles about tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1258945-71-9
di-tert-butyl 2,2'-(2-bromo-5-(4-nitrophenyl)pentylazanediyl)diacetate

: 1258946-46-1
tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

Guidance literature:: With silver perchlorate; In chloroform-d1; at -10 ℃; for 1h;

Reference yield:

: 1392222-48-8
tert-butyl 2-{[2-(tert-butoxy)-2-oxoethyl][2-iodo-5-(4-nitrophenyl)pentyl]amino}acetate

: 1258946-46-1
tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

Guidance literature:: With silver perchlorate; In acetonitrile; at -5 ℃; for 0.166667h;
DOI:10.1021/bc200696b

Reference yield:

: 1142811-83-3
{tert-butoxycarbonylmethyl-[1-hydroxymethyl-4-(4-nitrophenyl)butyl]amino}acetic acid tert-butyl ester

: 1258946-46-1
tert-butyl 2-[(1-{4,7-bis[2-(tert-butoxy)-2-oxoethyl]-1,4,7-triazonan-1-yl}-5-[4-nitrophenyl]pentan-2-yl)[2-(tert-butoxy)-2-oxoethyl]amino]acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 5 h / 0 - 20 °C

2: silver perchlorate / acetonitrile / 0.17 h / -5 °C

With 1H-imidazole; iodine; silver perchlorate; triphenylphosphine; In dichloromethane; acetonitrile;
DOI:10.1021/bc200696b