C₂₂H₃₃NO₆

Base Information

Chemical Name:C₂₂H₃₃NO₆
CAS No.:1257151-39-5
Molecular Formula:C₂₂H₃₃NO₆
Molecular Weight:407.507
Hs Code.:

C<sub>22</sub>H<sub>33</sub>NO<sub>6</sub>

Synonyms:C₂₂H₃₃NO₆

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Chemical Property of C₂₂H₃₃NO₆

Chemical Property:

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Technology Process of C₂₂H₃₃NO₆

There total 3 articles about C₂₂H₃₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67-56-1
methanol

: 1257151-37-3
C₂₇H₂₆N₄O₂

: 1257151-39-5
C₂₂H₃₃NO₆

Guidance literature:: C₂₇H₂₆N₄O₂; With hydrogenchloride; In water; acetic acid; for 22h; Reflux;

methanol; With thionyl chloride; at 0 - 20 ℃;

Reference yield:

: 1257151-33-9
C₂₁H₂₃NO₂

: 1257151-39-5
C₂₂H₃₃NO₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; hydrogen bromide; zinc dibromide / 72 h / 90 °C

1.2: 24 h / 20 °C

2.1: acetic acid; hydrogenchloride / 48 h / Reflux

2.2: 2 h / Reflux

With hydrogenchloride; hydrogen bromide; acetic acid; zinc dibromide; 2.2: |Fischer-Speier Esterification;
DOI:10.1039/c3sc51507a

Reference yield:

: 22445-41-6
3,5-dimethylphenyl iodide

: 1257151-39-5
C₂₂H₃₃NO₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 24 h / 90 °C

1.2: 24 h / 20 °C

2.1: acetic acid; hydrogen bromide; zinc dibromide / 72 h / 90 °C

2.2: 24 h / 20 °C

3.1: acetic acid; hydrogenchloride / 48 h / Reflux

3.2: 2 h / Reflux

With hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen bromide; acetic acid; triethylamine; zinc dibromide; 1.1: |Sonogashira Cross-Coupling / 3.2: |Fischer-Speier Esterification;
DOI:10.1039/c3sc51507a