(1-chloroprop-2-enyl)trimethyl silane

Base Information

• Chemical Name: (1-chloroprop-2-enyl)trimethyl silane
• CAS No.: 67965-28-0
• Molecular Formula: C₆H₁₃ClSi
• Molecular Weight: 148.708

Synonyms:(1-chloroprop-2-enyl)trimethyl silane

Chemical Property of (1-chloroprop-2-enyl)trimethyl silane

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of (1-chloroprop-2-enyl)trimethyl silane

There total 1 articles about (1-chloroprop-2-enyl)trimethyl silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

chloro-trimethyl-silane (75-77-4) + E/Z-1,3-Dichloropropene (542-75-6) → 1-chloro-3-trimethylsilylpropene (18187-39-8) + (1-chloroprop-2-enyl)trimethyl silane (67965-28-0)

Guidance literature:

With magnesium; ethylene dibromide; In tetrahydrofuran; diethyl ether; for 4h; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1246/bcsj.57.3017

Reference yield: 92.0%

(3,3-diethoxypropyl)benzene (6956-37-2) + (1-chloroprop-2-enyl)trimethyl silane (67965-28-0) → 1-chloro-4-ethoxy-6-phenyl-1-hexene (94397-52-1,94397-53-2)

Guidance literature:

With titanium tetrachloride; In dichloromethane; at -78 ℃; for 2h; Var_.reag.: SnCl₄, AlCl₃;

DOI:10.1246/cl.1984.1385

Reference yield: 90.0%

(1-chloroprop-2-enyl)trimethyl silane (67965-28-0) + aniline (62-53-3) → C12H19NSi (1134638-67-7)

Guidance literature:

With copper(l) chloride; In tert-butyl alcohol; for 0.333333h; Heating;

DOI:10.3184/030823407X237795

upstream raw materials:

chloro-trimethyl-silane

E/Z-1,3-Dichloropropene

Downstream raw materials:

(E)-6-Chloro-1-phenyl-hex-5-en-3-ol

((E)-4-Chloro-1-methoxy-but-3-enyl)-benzene

1-chloro-4-ethoxy-6-phenyl-1-hexene

((E)-7-Chloro-4-ethoxy-hept-6-enyl)-benzene

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